Very high fluence nitrogen implantations in metals studied by Rutherford Backscattering Spectrometry

J. Cruz, H. Silva, J. Lopes, J. Rocha, A. P. Jesus

Research output: Contribution to journalConference article

1 Citation (Scopus)

Abstract

This paper reports a study of 14N+ implanted Ti and Zr films analysed by Rutherford Backscattering Spectrometry (RBS). The fluences ranged from 4.0-10.0 × 1017 atoms·cm-2 and energies of 15-20 keV. Here, the nitrogen depth distributions were obtained simultaneously and independently for each RBS spectrum from the direct nitrogen signal and from the reduction of the backscattered yield from Ti and Zr (deficiency method). Fits to the RBS spectra show that the deficiency method clearly underestimates the 14N yield by 32% for Ti (and 45% for Zr) when compared to the direct nitrogen signal. This discrepancy reduces to 23% for Ti (and 43% for Zr) when the presence of nitrogen bubbles are simulated in the fits.

Original languageEnglish
Pages (from-to)169-173
JournalSurface and Coatings Technology
Volume355
DOIs
Publication statusPublished - 15 Dec 2018
EventInternational Conference on Surface Modification of Materials by Ion Beams (SMMIB) - Lisbon, Portugal
Duration: 9 Jul 201714 Jul 2017

Fingerprint

Rutherford backscattering spectroscopy
Spectrometry
implantation
backscattering
fluence
Nitrogen
Metals
nitrogen
metals
spectroscopy
bubbles
energy

Keywords

  • Deficiency method
  • Nitrogen implantation
  • RBS
  • Stopping power

Cite this

@article{efe0ebeb2ef94313add6e61302bd6efd,
title = "Very high fluence nitrogen implantations in metals studied by Rutherford Backscattering Spectrometry",
abstract = "This paper reports a study of 14N+ implanted Ti and Zr films analysed by Rutherford Backscattering Spectrometry (RBS). The fluences ranged from 4.0-10.0 × 1017 atoms·cm-2 and energies of 15-20 keV. Here, the nitrogen depth distributions were obtained simultaneously and independently for each RBS spectrum from the direct nitrogen signal and from the reduction of the backscattered yield from Ti and Zr (deficiency method). Fits to the RBS spectra show that the deficiency method clearly underestimates the 14N yield by 32{\%} for Ti (and 45{\%} for Zr) when compared to the direct nitrogen signal. This discrepancy reduces to 23{\%} for Ti (and 43{\%} for Zr) when the presence of nitrogen bubbles are simulated in the fits.",
keywords = "Deficiency method, Nitrogen implantation, RBS, Stopping power",
author = "J. Cruz and H. Silva and J. Lopes and J. Rocha and Jesus, {A. P.}",
year = "2018",
month = "12",
day = "15",
doi = "10.1016/j.surfcoat.2018.01.042",
language = "English",
volume = "355",
pages = "169--173",
journal = "Surface & Coatings Technology",
issn = "0257-8972",
publisher = "Elsevier Science B.V., Amsterdam.",

}

Very high fluence nitrogen implantations in metals studied by Rutherford Backscattering Spectrometry. / Cruz, J.; Silva, H.; Lopes, J.; Rocha, J.; Jesus, A. P.

In: Surface and Coatings Technology, Vol. 355, 15.12.2018, p. 169-173.

Research output: Contribution to journalConference article

TY - JOUR

T1 - Very high fluence nitrogen implantations in metals studied by Rutherford Backscattering Spectrometry

AU - Cruz, J.

AU - Silva, H.

AU - Lopes, J.

AU - Rocha, J.

AU - Jesus, A. P.

PY - 2018/12/15

Y1 - 2018/12/15

N2 - This paper reports a study of 14N+ implanted Ti and Zr films analysed by Rutherford Backscattering Spectrometry (RBS). The fluences ranged from 4.0-10.0 × 1017 atoms·cm-2 and energies of 15-20 keV. Here, the nitrogen depth distributions were obtained simultaneously and independently for each RBS spectrum from the direct nitrogen signal and from the reduction of the backscattered yield from Ti and Zr (deficiency method). Fits to the RBS spectra show that the deficiency method clearly underestimates the 14N yield by 32% for Ti (and 45% for Zr) when compared to the direct nitrogen signal. This discrepancy reduces to 23% for Ti (and 43% for Zr) when the presence of nitrogen bubbles are simulated in the fits.

AB - This paper reports a study of 14N+ implanted Ti and Zr films analysed by Rutherford Backscattering Spectrometry (RBS). The fluences ranged from 4.0-10.0 × 1017 atoms·cm-2 and energies of 15-20 keV. Here, the nitrogen depth distributions were obtained simultaneously and independently for each RBS spectrum from the direct nitrogen signal and from the reduction of the backscattered yield from Ti and Zr (deficiency method). Fits to the RBS spectra show that the deficiency method clearly underestimates the 14N yield by 32% for Ti (and 45% for Zr) when compared to the direct nitrogen signal. This discrepancy reduces to 23% for Ti (and 43% for Zr) when the presence of nitrogen bubbles are simulated in the fits.

KW - Deficiency method

KW - Nitrogen implantation

KW - RBS

KW - Stopping power

UR - http://www.scopus.com/inward/record.url?scp=85041556664&partnerID=8YFLogxK

U2 - 10.1016/j.surfcoat.2018.01.042

DO - 10.1016/j.surfcoat.2018.01.042

M3 - Conference article

VL - 355

SP - 169

EP - 173

JO - Surface & Coatings Technology

JF - Surface & Coatings Technology

SN - 0257-8972

ER -