Tautomerism in 5-aminotetrazole investigated by core-level photoelectron spectroscopy and ΔsCF calculations

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Abstract

The C 1s and N 1s photoelectron spectra of gas-phase 5-aminotetrazole (5ATZ) were recorded using synchrotron radiation, with the aim of evaluating 1H/2H tautomer population ratios. The core-electron binding energies (CEBEs) were estimated from computational results, using the delta self-consistent-field (ΔSCF) approach. Simulated spectra were generated using these CEBEs and the results from Gaussian-n (Gn, n = 1, 2 and 3) and Complete Basis Set (CBS-4M and CBS-Q) methods. Results reveal the almost exclusive predominance of the 2H-tautomer, with a 1H/2H ratio of ca. 0.12/0.88, taken from a gross analysis of the XPS C 1s spectrum, recorded at 365 K.

Original languageEnglish
Pages (from-to)13-17
Number of pages5
JournalJournal of Electron Spectroscopy and Related Phenomena
Volume185
Issue number1-2
DOIs
Publication statusPublished - Mar 2012

Keywords

  • 5-Aminotetrazole
  • Synchrotron
  • Tautomerism
  • XPS

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