TY - JOUR
T1 - Ni-based superalloy 718 fabricated by arc-based directed energy deposition
T2 - an experimentally-based strengthening mechanisms analysis
AU - Farias, Francisco Werley Cipriano
AU - Duarte, Valdemar Rebelo
AU - Filho, João da Cruz Payão
AU - Figueiredo, Arthur Ribeiro
AU - Schell, Norbert
AU - Maawad, Emad
AU - Fonseca, Fabio Machado Alves da
AU - Cormier, Jonathan
AU - Ramirez, Antonio J.
AU - Santos, Telmo G.
AU - Oliveira, J. P.
N1 - info:eu-repo/grantAgreement/FCT/Financiamento do Plano Estratégico de Unidades de I&D - 2019/UID%2FEMS%2F00667%2F2019/PT#
info:eu-repo/grantAgreement/FCT/6817 - DCRRNI ID/LA%2FP%2F0037%2F2020/PT#
info:eu-repo/grantAgreement/FCT/6817 - DCRRNI ID/UIDP%2F50025%2F2020/PT#
info:eu-repo/grantAgreement/FCT/6817 - DCRRNI ID/UIDP%2F50025%2F2020/PT#
info:eu-repo/grantAgreement/FCT/Concurso de avaliação no âmbito do Programa Plurianual de Financiamento de Unidades de I&D (2017%2F2018) - Financiamento Base/UIDB%2F50025%2F2020/PT#
info:eu-repo/grantAgreement/FCT/OE/2022.13870.BD/PT#
info:eu-repo/grantAgreement/EC/H2020/730872/EU#
info:eu-repo/grantAgreement/FCT/Concurso de avaliação no âmbito do Programa Plurianual de Financiamento de Unidades de I&D (2017%2F2018) - Financiamento Base/UIDB%2F50025%2F2020/PT#
Funding Information:
Authors acknowledge the Portuguese Fundação para a Ciência e a Tecnologia (FCT – MCTES) for its financial support via the project UID/EMS/00667/2019 (UNIDEMI). JPO acknowledges funding by national funds from FCT - Fundação para a Ciência e a Tecnologia, I.P., in the scope of the projects LA/P/0037/2020, UIDP/50025/2020 and UIDB/50025/2020 of the Associate Laboratory Institute of Nanostructures, Nanomodelling and Nanofabrication – i3N. Funding of CENIMAT/i3N by national funds through the FCT-Fundação para a Ciência e a Tecnologia, I.P., within the scope of Multiannual Financing of R&D Units, reference UIDB/50025/2020–2023 is also acknowledge. FWCF acknowledges Fundação para a Ciência e a Tecnologia (FCT-MCTES) for funding the Ph.D. Grant 2022.13870.BD. The authors acknowledge DESY (Hamburg, Germany), a member of the Helmholtz Association HGF, for the provision of experimental facilities. Beamtime was allocated for proposal I-20210986 EC. The research leading to this result has been supported by the project CALIPSOplus under the Grant Agreement 730872 from the EU Framework Programme for Research and Innovation HORIZON 2020.
Publisher Copyright:
© 2025 The Authors
PY - 2025/9
Y1 - 2025/9
N2 - The present work describes and quantitatively assesses the strengthening mechanisms in Inconel 718 fabricated by arc-based DED (IN718 arc-based DED) through an experimentally-based approach. IN718 arc-based DED (in the as-built condition) showed a typical coarse (millimetric-sized grains) and oriented (cube texture) microstructure with a significant quantity of interdendritic eutectics (Laves and MC-type carbides). After heat treatment (1100 °C/2 h + aging), these eutectics were partially dissolved; however, the original grain size and crystallographic texture aspects were not altered. In addition, the heat treatment promoted a notorious γ′′ (Ni3Nb) and γ′ (Ni3(Al, Ti)) phases content (∼17 and 5 %, respectively), which results in superior room temperature tensile strength despite the aforementioned non-optimized microstructure. The grain size, dislocation density, precipitation content and morphology, and alloying elements in solid solution were experimentally measured and utilized as input data for a quantitative assessment of the strengthening mechanisms. This analysis concludes that the linear dependence of the majority of the strengthening mechanisms on the Taylor factor predominantly promoted the yield strength anisotropy. Furthermore, as expected, it is evidenced that the precipitation strengthening mechanism governs the final strength of IN718 arc-based DED.
AB - The present work describes and quantitatively assesses the strengthening mechanisms in Inconel 718 fabricated by arc-based DED (IN718 arc-based DED) through an experimentally-based approach. IN718 arc-based DED (in the as-built condition) showed a typical coarse (millimetric-sized grains) and oriented (cube texture) microstructure with a significant quantity of interdendritic eutectics (Laves and MC-type carbides). After heat treatment (1100 °C/2 h + aging), these eutectics were partially dissolved; however, the original grain size and crystallographic texture aspects were not altered. In addition, the heat treatment promoted a notorious γ′′ (Ni3Nb) and γ′ (Ni3(Al, Ti)) phases content (∼17 and 5 %, respectively), which results in superior room temperature tensile strength despite the aforementioned non-optimized microstructure. The grain size, dislocation density, precipitation content and morphology, and alloying elements in solid solution were experimentally measured and utilized as input data for a quantitative assessment of the strengthening mechanisms. This analysis concludes that the linear dependence of the majority of the strengthening mechanisms on the Taylor factor predominantly promoted the yield strength anisotropy. Furthermore, as expected, it is evidenced that the precipitation strengthening mechanism governs the final strength of IN718 arc-based DED.
KW - Additive manufacturing
KW - Directed energy deposition
KW - Inconel 718
KW - Strengthening mechanism
KW - Wire and arc additive manufacturing
UR - http://www.scopus.com/inward/record.url?scp=105005107910&partnerID=8YFLogxK
UR - https://www.webofscience.com/wos/woscc/full-record/WOS:001496071500001
U2 - 10.1016/j.msea.2025.148417
DO - 10.1016/j.msea.2025.148417
M3 - Article
AN - SCOPUS:105005107910
SN - 0921-5093
VL - 939
SP - 1
EP - 14
JO - Materials Science and Engineering: A
JF - Materials Science and Engineering: A
M1 - 148417
ER -