Golden glazes analysis by PIGE and PIXE techniques

M. Fonseca; H. Luís; N. Franco; M. A. Reis; P. C. Chaves; A. Taborda; J. Cruz; D. Galaviz; N. Fernandes; P. Vieira; J. P. Ribeiro; A. P. Jesus

doi:10.1016/j.nimb.2011.04.060

Golden glazes analysis by PIGE and PIXE techniques

M. Fonseca, H. Luís, N. Franco, M. A. Reis, P. C. Chaves, A. Taborda, J. Cruz, D. Galaviz, N. Fernandes, P. Vieira, J. P. Ribeiro, A. P. Jesus

DF – Departamento de Física

Research output: Contribution to journal › Conference article › peer-review

3 Citations (Scopus)

Abstract

We present the analysis performed on the chemical composition of two golden glazes available in the market using the PIGE and PIXE techniques at the ITN ion beam laboratory. The analysis of the light elements was performed using the Emitted Radiation Yield Analysis (ERYA) code, a standard-free method for PIGE analysis on thick samples. The results were compared to those obtained on an old glaze. Consistently high concentrations of lead and sodium were found in all analyzed golden glazes. The analysis of the samples pointed to Mo and Co as the specific elements responsible of the gold colour at the desired temperature, and allowed Portuguese ceramists to produce a golden glaze at 997 °C. Optical reflection spectra of the glazes are given, showing that the produced glaze has a spectrum similar to the old glaze. Also, in order to help the ceramists, the unknown compositions of four different types of frits (one of the components of glazes) were analysed.

Original language	English
Pages (from-to)	3060-3062
Number of pages	3
Journal	Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms
Volume	269
Issue number	24
DOIs	https://doi.org/10.1016/j.nimb.2011.04.060
Publication status	Published - 15 Dec 2011
Event	10th European Conference on Accelerators in Applied Research and Technology (ECAART) - Athens, Greece Duration: 13 Sept 2010 → 17 Sept 2010

Keywords

Optical reflection spectroscopy
PIGE
PIXE
Quantitative thick samples analysis

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Fonseca, M., Luís, H., Franco, N., Reis, M. A., Chaves, P. C., Taborda, A., Cruz, J., Galaviz, D., Fernandes, N., Vieira, P., Ribeiro, J. P., & Jesus, A. P. (2011). Golden glazes analysis by PIGE and PIXE techniques. Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, 269(24), 3060-3062. https://doi.org/10.1016/j.nimb.2011.04.060

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title = "Golden glazes analysis by PIGE and PIXE techniques",

abstract = "We present the analysis performed on the chemical composition of two golden glazes available in the market using the PIGE and PIXE techniques at the ITN ion beam laboratory. The analysis of the light elements was performed using the Emitted Radiation Yield Analysis (ERYA) code, a standard-free method for PIGE analysis on thick samples. The results were compared to those obtained on an old glaze. Consistently high concentrations of lead and sodium were found in all analyzed golden glazes. The analysis of the samples pointed to Mo and Co as the specific elements responsible of the gold colour at the desired temperature, and allowed Portuguese ceramists to produce a golden glaze at 997 °C. Optical reflection spectra of the glazes are given, showing that the produced glaze has a spectrum similar to the old glaze. Also, in order to help the ceramists, the unknown compositions of four different types of frits (one of the components of glazes) were analysed.",

keywords = "Optical reflection spectroscopy, PIGE, PIXE, Quantitative thick samples analysis",

author = "M. Fonseca and H. Lu{\'i}s and N. Franco and Reis, {M. A.} and Chaves, {P. C.} and A. Taborda and J. Cruz and D. Galaviz and N. Fernandes and P. Vieira and Ribeiro, {J. P.} and Jesus, {A. P.}",

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Fonseca, M, Luís, H, Franco, N, Reis, MA, Chaves, PC, Taborda, A, Cruz, J, Galaviz, D, Fernandes, N, Vieira, P, Ribeiro, JP & Jesus, AP 2011, 'Golden glazes analysis by PIGE and PIXE techniques', Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, vol. 269, no. 24, pp. 3060-3062. https://doi.org/10.1016/j.nimb.2011.04.060

TY - JOUR

T1 - Golden glazes analysis by PIGE and PIXE techniques

AU - Fonseca, M.

AU - Luís, H.

AU - Franco, N.

AU - Reis, M. A.

AU - Chaves, P. C.

AU - Taborda, A.

AU - Cruz, J.

AU - Galaviz, D.

AU - Fernandes, N.

AU - Vieira, P.

AU - Ribeiro, J. P.

AU - Jesus, A. P.

PY - 2011/12/15

Y1 - 2011/12/15

N2 - We present the analysis performed on the chemical composition of two golden glazes available in the market using the PIGE and PIXE techniques at the ITN ion beam laboratory. The analysis of the light elements was performed using the Emitted Radiation Yield Analysis (ERYA) code, a standard-free method for PIGE analysis on thick samples. The results were compared to those obtained on an old glaze. Consistently high concentrations of lead and sodium were found in all analyzed golden glazes. The analysis of the samples pointed to Mo and Co as the specific elements responsible of the gold colour at the desired temperature, and allowed Portuguese ceramists to produce a golden glaze at 997 °C. Optical reflection spectra of the glazes are given, showing that the produced glaze has a spectrum similar to the old glaze. Also, in order to help the ceramists, the unknown compositions of four different types of frits (one of the components of glazes) were analysed.

AB - We present the analysis performed on the chemical composition of two golden glazes available in the market using the PIGE and PIXE techniques at the ITN ion beam laboratory. The analysis of the light elements was performed using the Emitted Radiation Yield Analysis (ERYA) code, a standard-free method for PIGE analysis on thick samples. The results were compared to those obtained on an old glaze. Consistently high concentrations of lead and sodium were found in all analyzed golden glazes. The analysis of the samples pointed to Mo and Co as the specific elements responsible of the gold colour at the desired temperature, and allowed Portuguese ceramists to produce a golden glaze at 997 °C. Optical reflection spectra of the glazes are given, showing that the produced glaze has a spectrum similar to the old glaze. Also, in order to help the ceramists, the unknown compositions of four different types of frits (one of the components of glazes) were analysed.

KW - Optical reflection spectroscopy

KW - PIGE

KW - PIXE

KW - Quantitative thick samples analysis

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U2 - 10.1016/j.nimb.2011.04.060

DO - 10.1016/j.nimb.2011.04.060

M3 - Conference article

AN - SCOPUS:81855213157

SN - 0168-583X

VL - 269

SP - 3060

EP - 3062

JO - Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms

JF - Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms

IS - 24

T2 - 10th European Conference on Accelerators in Applied Research and Technology (ECAART)

Y2 - 13 September 2010 through 17 September 2010

ER -

Golden glazes analysis by PIGE and PIXE techniques

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Keywords

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