Fast Synthesis of N-Acylhydrazones Employing a Microwave Assisted Neat Protocol

Maria Teresa Barros; Marta Morais Saraiva de Andrade

doi:10.1021/cc9001444

Fast Synthesis of N-Acylhydrazones Employing a Microwave Assisted Neat Protocol

Maria Teresa Barros, Marta Morais Saraiva de Andrade

Research output: Contribution to journal › Article › peer-review

26 Citations (Scopus)

Abstract

A variety of N-acylhydrazones were synthesized Under microwave irradiation within 2.5-10 min, starting from benzo, salicyloyl, and isonicotinic hydrazides. The protocol developed employs microwave irradiation in the absence of solvents and catalysts, leading to high yields. The results are reproducible in a 500 mg to 5 g scale.

Original language	Unknown
Pages (from-to)	245-247
Journal	Journal Of Combinatorial Chemistry
Volume	12
Issue number	2
DOIs	https://doi.org/10.1021/cc9001444
Publication status	Published - 1 Jan 2010

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10.1021/cc9001444

Cite this

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title = "Fast Synthesis of N-Acylhydrazones Employing a Microwave Assisted Neat Protocol",

abstract = "A variety of N-acylhydrazones were synthesized Under microwave irradiation within 2.5-10 min, starting from benzo, salicyloyl, and isonicotinic hydrazides. The protocol developed employs microwave irradiation in the absence of solvents and catalysts, leading to high yields. The results are reproducible in a 500 mg to 5 g scale.",

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N2 - A variety of N-acylhydrazones were synthesized Under microwave irradiation within 2.5-10 min, starting from benzo, salicyloyl, and isonicotinic hydrazides. The protocol developed employs microwave irradiation in the absence of solvents and catalysts, leading to high yields. The results are reproducible in a 500 mg to 5 g scale.

AB - A variety of N-acylhydrazones were synthesized Under microwave irradiation within 2.5-10 min, starting from benzo, salicyloyl, and isonicotinic hydrazides. The protocol developed employs microwave irradiation in the absence of solvents and catalysts, leading to high yields. The results are reproducible in a 500 mg to 5 g scale.

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KW - adducts

KW - complexes

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